Meddelelser KEMISK INSTITUT. Ph.d.-forsvar: Miljøvenlig cement udviklet ved fluorid-ion mineralisering af Portland cement
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1 Index for nr. 33 S 267 Ph.D. forsvar: Thuan T. Tran S 268 Ph.D. forsvar: Grethe Vestergaard Jensen S 269 Ph.D. forsvar: Kasper Kristensen S 270 Kandidatårseksamen: Sidsel Dahl Schrøder S 271 Kandidatårseksamen: Anja Funch Brøgger S 272 Kandidatårseksamen: Anders Valdemar Edhager S 273 inano Lecture: Professor, Dr. Hellmut Eckert S 274 Specialized inano Lecture: Dr. Jörg H. Kleinschmidt
2 Meddelelser KEMISK INSTITUT 43. årgang nr. 33 AARHUS UNIVERSITET 20. oktober 2011 Ph.d.-forsvar: Miljøvenlig cement udviklet ved fluorid-ion mineralisering af Portland cement Portland cement er et af samfundets vigtigste byggematerialer med en årlig verdensproduktion på 3.3 mia. tons i Det forventes at produktionen vil fordobles inden år 2050, især på grund af det stigende behov for bygninger og udvikling af infra-strukturer i Kina, Indien og i en lang række udviklingslande. Dette repræsenterer en kæmpe udfordring for cementindustrien, da cement-produktionen i dag allerede er ansvarlig for ca. 5 % af den menneskeskabte CO 2 udledning. En signifikant reduktion i denne CO 2 -emission kan bl.a. opnås ved delvist at erstatte Portland cement med alternative materialer såsom forebehandlede ler-mineraler. Cand. Scient. Thuan T. Tran har i sit ph.d. projekt forsket i udviklingen af en ny cement type, hvor 30 % af den traditionelle Portland cement er erstattet med alternative materialer baseret på lermineraler uden at cementens styrke og holdbarhed er reduceret. Thuan T. Trans bidrag til dette mål har været at optimere Portland cementens kemiske sammensætning, således at der opnås en forøget reaktivitet for cement-faserne. Et hovedprojekt i ph.d. studiet har også været at udvikle faststof dobbelt-resonans kerne-magnetisk resonans (NMR) eksperimenter til strukturkarakterisering af cement-materialer. Thuan T. Tran har med disse eksperimenter opnået ny strukturel information om gæst-ioner, specielt fluorid-ioner, indbygget i cementmineralerne, hvilket er udnyttet i optimeringen af cementens kemiske sammensætning. Ph.d. studiet er udført ved Interdisciplinært Nanoscience Center, inano, og Institut for Kemi, Aarhus Universitet i samarbejde med Aalborg Portland A/S og med økonomisk støtte fra Højteknologifonden. Grafen viser trykstyrke som funktion af hydratiseringstid for den fluorid-ion mineraliserede cement, der blev udviklet i ph.d. projektet s amt for en konvent ionel hvid Portland cement. Det ses tydeligt, at der opnås en signifikant højere trykstyrke for den fluorid- mineraliserede cement. Tid: Fredag den 21. oktober 2011 kl Sted: Auditorium I (bygning 1514 lokale 213), Institut for Kemi, Aarhus Universitet. Afhandlingens titel: Fluoride Mineralization of Portland cement. Applications of Double-Resonance NMR Spectroscopy in Structural Investigations of Guest Ions in Cement Phases. Kontaktinfo: Thuan T. Tran, thuantran@chem.au.dk, tlf: / Bedømmelsesudvalg: Professor Hellmut Eckert, Westfälische Wilhelm-Universität Münster, Institut für Physikalische Chemie, Münster, Tyskland. R&D Project Manager Ebbe Skyum Jøns, FLSmidth A/S, Valby, Danmark. Professor Niels Chr. Nielsen, (formand) inano og Institut for Kemi, Aarhus Universitet, Aarhus, Danmark. Vejleder: Lektor Jørgen Skibsted, inano og Institut for Kemi, Aarhus Universitet, Aarhus, Danmark. Medvejleder: Chief Scientist Duncan Herfort, Aalborg Portland A/S, Aalborg, Danmark. Sprog: Ph.d.-afhandlingen forsvares på engelsk. Forsvaret er offentligt. Afhandlingen ligger til gennemsyn hos Aarhus Graduate School of Science, AGSoS, Ny Munkegade 120, bygning 1521, lokale
3 MOLEKYLER DER SAMLER SIG I AVANCEREDE NANOSTRUKTURER - HVORFOR OG HVORDAN? Ph.d.-forsvar, fredag den 14. oktober Cand.scient. Grethe Vestergaard Jensen. I løbet af sit ph.d.-studium har Grethe Vestergaard Jensen forsket i molekyler, der er 'programmeret', så de samler sig i veldefinerede strukturer. Dette gælder f.eks. for sæbemolekyler og større molekyler sammensat af to forskellige polymerblokke. I vand danner disse molekyler små aggregater kaldet miceller, der kan have et væld af forskellige størrelser og former (runde, aflange, flade) afhængigt af molekylernes kemiske struktur. De har mange forskellige anvendelser som tensider, stabilisatorer og emulgatorer, både inden for rengøring, personlig pleje, i olieindustrien, fødevarer og i medicin RIKKE J. LJUNGMANN I afhandlingen vises det, hvordan micellernes struktur kan bestemmes ved hjælp af spredning af røntgenstråling. For at forstå hvad der er afgørende for, hvilken struktur der dannes, sammenlignes resultaterne med forskellige teoretiske forudsigelser. Når der tilsættes salt, eller når opløsningerne blandes med andre sæbemolekyler, kan micellerne ændre form, eller nye miceller kan dannes. Dette forgår meget hurtigt, i løbet af brøkdele af et sekund. Ved brug af høj-intensiv røntgenstråling fra en synkrotronkilde, kan ændringerne følges. Dette har givet ny viden om de molekylære mekanismer, der er involveret i dannelsen af miceller. Twitter Facebook Synes godt om Ph.d.-studiet er gennemført ved Interdisciplinært Nanoscience Center, inano, under Science and Technology ved Aarhus Universitet. Grethe Vestergaard Jensen Tid: Fredag den 14. oktober 2011 kl Sted: Auditorium D2, Institut for Matematik, Aarhus Universitet Afhandlingens titel: Scattering Studies of Micelles in Solution. Structure, Formation, and Rearrangement of Micelles Kontaktinfo: Grethe Vestergaard Jensen, inagvj@inano.au.dk Bedømmelsesudvalg: Professor, Dr. Stefan Egelhaaf, Lehrstuhl für Physik der weichen Materie, Heinrich-Heine-Universität, Düsseldorf, Tyskland Professor Kell Mortensen, Head of Biophysics Group, Department of Natural Sciences, Faculty of Life Sciences, Københavns Universitet Professor Niels Chr. Nielsen (formand), inano og Institut for Kemi, Aarhus Universitet Hovedvejleder: Professor Jan Skov Pedersen, inano og Institut for Kemi, Aarhus Universitet Sprog: Ph.d.-afhandlingen forsvares på engelsk. Forsvaret er offentligt. Afhandlingen ligger til gennemsyn hos Graduate School of Science and Technology, GSST, Ny Munkegade 120, bygning 1521, lokale 112. Ph. D. Forsvar Forskellige geometrier af molekylerne giver forskellige nanostrukturer HENVENDELSE OM DENNE SIDES INDHOLD: IDA MARIE GERDES REVIDERET Science and Technology mail@science.au.dk CVR-nr: Henvendelser til webredaktør Aarhus Universitet Tlf: P-nr: Ny Munkegade 120 Fax: EAN-nr: Aarhus C Stedkode: 51111
4 HIGH-ACCURACY COMPUTER CALCULATIONS ON LARGE MOLECULES PhD defence, Friday 21 October Kasper Kristensen ANNE HAVE LIETZEN Computer calculations on molecules often supplement experimental studies and may to some extent also replace expensive or potentially dangerous experiments. The main challenge for traditional high-accuracy methods is that the time for a calculation increases dramatically with system size (for example, a high-precision calculation of insulin would take several million years!). This makes it impossible to carry out accurate theoretical studies of, for example, large biological molecules with potential applications in the pharmaceutical industry i.e. how a drug binds to a protein. Twitter Facebook Synes godt om During his PhD studies, Kasper Kristensen investigated how high-accuracy quantum mechanical models can be reformulated to make them applicable to large molecules (e.g. proteins). The basic formulations have been implemented, thereby providing the foundation for future high-accuracy theoretical studies of biological molecules, for example. Kasper Kristensen Time: Friday 21 October 2011 at Place: Lecture Theatre VI, building 1510, room 213 Title of dissertation: Self-Consistent Field Response Theory and Coupled-Cluster Theory Contact information: Kasper Kristensen, kasperk@chem.au.dk Members of the assessment committee: Professor Hans-Joachim Werner, University of Stuttgart, Germany Professor Jack Simons, University of Utah, USA Associate Professor Ove Christensen, Department of Chemistry, Aarhus University Supervisor: Professor Poul Jørgensen, Department of Chemistry, Aarhus University Language: The dissertation will be defended in English The defence is public. The dissertation is available for reading at the Graduate School of Science and Technology / GSST, Ny Munkegade 120, building 1521, room 112. Ph. D. Forsvar Illustration of insulin. To describe a molecule of this size, it is necessary to describe local physical effects without having to consider the whole molecule. The core of the project is to do this using local functions, such as the yellow/green mushroom in the left part of the image. COMMENTS ON CONTENT: IDA MARIE GERDES REVISED Science and Technology mail@science.au.dk CVR no: Contact web editor Aarhus University Tel: P no: Ny Munkegade 120 Fax: EAN no: DK-8000 Aarhus C Budget code: Denmark
5 O P S L A G NATURVIDENSKABELIG KANDIDATEKSAMEN SOMMER 2011 KEMI Kandidatårseksamen: Sidsel Dahl Schrøder Mundtlig eksamen: Torsdag den , kl Eksamen afholdes: Aud. I
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8 inano lecture of the week - open to all Professor, Dr. Hellmut Eckert Institut für Physikalische Chemie Westfalhlische Wilhelms-Universität Münster, Germany Title: Time: New Magnetic Resonance Approaches Towards the Structural Characterization of Luminescent Ceramic Materials Friday 21 October 2011, at 10:15am Coffee and bread will be served from 10am Location: Aud I, Department of Chemistry ( ) Abstract: Glasses and vitroceramics based have been introduced as excellent alternatives to single crystalline host materials for luminescent rare-earth ions with special laser applications. To optimize the luminescent properties of these materials, detailed structural information regarding the local environment of the rare-earth species is essential. This characterization must include the distribution of the rare earth ions over the different crystalline and amorphous components present. While solid state nuclear magnetic resonance (NMR) is in general a promising tool for such purposes, unfortunately, the rare-earth ions themselves cannot be studied by NMR due to their paramagnetism. To overcome this difficulty, we have developed a comprehensive examination strategy consisting of (a) the use of diamagnetic mimics such as 45 Sc and 89 Y NMR [1], (b) the quantification of paramagnetic broadening effects imparted by the rare-earth ions upon the solid state NMR spectra of framework atoms [2], and (c) the direct study of electron-nuclear interactions as probed by electron spin echo envelope modulation (ESEEM) spectroscopy [3]. Results will be presented for a range of rare-earth containing aluminoborate and phosphate glasses and ceramics, and extensions to other laser ceramic systems will be discussed. References: [1] H. Deters, H.; A. S. S. de Camargo, C. N. Santos, C. R. Ferrari, A. C. Hernandes, A. Ibanez, M. T. Rinke, H. Eckert, J. Phys. Chem. C 113, (2009). [2] H. Deters, A. S. S. de Camargo, C. N. Santos, H. Eckert, J. Phys. Chem. C 114, (2010). [3] H. Deters, J. F. de Lima, C. J. Magon, A. S. S. de Camargo, H. Eckert, Phys. Chem. Chem. Phys. 2011, in press.
9 Specialized inano lecture - open to all Dr Jörg H. Kleinschmidt Department of Biology University of Konstanz Konstanz, Germany Title: Role of folding factors from the periplasm of E.coli in insertion and folding of a β-barrel membrane protein into lipid bilayers. Time: Monday 24 October 2011, at 11:15 Location: , Department of Physics Abstract: Folding and insertion of outer membrane proteins (OMPs) of Gram-negative bacteria are not well understood. Biosynthesized in the cytosol, OMPs are translocated via the SecYEG translocon across the plasma membrane into the periplasm, where the leader peptidase cleaves their signal sequence. The subsequent transport and insertion into the outer membrane (OM) are mediated by several folding factors. Once inserted into the OM, the transmembrane domains of most OMPs form highly stable β-barrel structures, composed of an even number of β-strands, ranging from 8 to 24. Several proteins have been isolated from the periplasm, which prevent aggregation of unfolded OMPs in aqueous solution and in the periplasm. Depletion of these molecular chaperones in cells leads to lower concentrations of the OMPs in the OM, indicating that chaperones are important for OMP transport and/or OMP insertion. However, the periplasmic chaperones are not essential for cell survival. In contrast, the β-barrel assembly machinery complex (BAM-complex), which is part of the OM, is essential for OMP assembly and OM-biogenesis. For the outer membrane protein A as a client OMP, I present biophysical data for the roles of the periplasmic chaperones Skp, FkpA, and SurA and for the role of the core protein of the BAM complex, BamA.
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